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Beilstein J. Org. Chem. 2011, 7, 1288–1293, doi:10.3762/bjoc.7.149
Graphical Abstract
Figure 1: Hastelloy-made micromixer (MiChS β-150H).
Figure 2: Hastelloy-made microextraction unit.
Figure 3: Acid-tolerant microflow system used for the Koch–Haaf reaction.
Scheme 1: Synthesis of 1-adamantanecarboxylic acid (2a) in a microflow system.
Scheme 2: Koch–Haaf reaction of 1b and 1c in a microflow system.
Scheme 3: Multigram scale flow synthesis of 1-adamantanecarboxylic acid (2a).